 |
(Result with barometric collection)
| |
Obs/Corr |
%/min |
|
Evap. |
Heat |
| % |
oC |
or time |
% |
oC |
W |
| IBP |
69.3 |
4min41s |
IBP |
69.3 |
|
| 1 |
96.7 |
|
1 |
88.6 |
180 |
| 2 |
113.7 |
|
2 |
105.5 |
180 |
| 3 |
127.2 |
|
3 |
121.6 |
191 |
| 4 |
136.3 |
|
4 |
132.0 |
192 |
| 5 |
142.6 |
107s |
5 |
139.9 |
178 |
| 10 |
157.9 |
6.6 |
10 |
157.3 |
113 |
| 15 |
169.7 |
5.6 |
15 |
168.5 |
80 |
| 20 |
178.9 |
4.2 |
20 |
178.2 |
105 |
| 25 |
186.1 |
4.2 |
25 |
185.1 |
108 |
| 30 |
196.1 |
4.2 |
30 |
195.4 |
127 |
| 35 |
207.9 |
4.2 |
35 |
206.4 |
142 |
| 40 |
222.5 |
4.0 |
40 |
220.6 |
176 |
| 45 |
241.4 |
4.1 |
45 |
239.4 |
196 |
| 50 |
260.3 |
4.4 |
50 |
258.5 |
204 |
| 55 |
274.6 |
4.6 |
55 |
273.1 |
207 |
| 60 |
289.6 |
4.3 |
60 |
287.8 |
221 |
| 65 |
304.6 |
4.1 |
65 |
302.8 |
253 |
| 70 |
320.6 |
4.2 |
70 |
318.7 |
278 |
| 75 |
336.5 |
4.2 |
75 |
334.8 |
304 |
| 80 |
350.2 |
4.5 |
80 |
349.1 |
320 |
| 85 |
363.1 |
4.0 |
85 |
361.9 |
360 |
| 90 |
378.9 |
3.9 |
90 |
377.1 |
428 |
| 91 |
|
|
|
|
|
| STOP
90.2% 380.2oC |
|
| Percent recovery |
: 93.4 % |
| Percent residue |
: 6.1 % |
| Total recovery |
: 99.5 % |
| Corrected loss |
: 0.5 % |
| Corrected total recovery |
: 99.5 % |
| Ambient temperature |
: 24 oC |
| Atmospheric pressure |
: 101.7 kPa |
| Condenser bath temp. |
: 23 oC |
| Graduate chamber temp. |
: 23 oC |
|
| Volume at 250.0 oC |
47.1 % |
47.6 % |
| Volume at 350.0 oC |
79.9 % |
80.4 % |
| Volume at 360.0 oC |
83.7 % |
84.2 % |
| Volume at 370.0 oC |
87.3 % |
87.8 % |
|
